|
No
|
CRITERIA
|
TEST METHOD
|
LOD (Unit)
|
|
I. ORGANOLEPTIC AND PHYSICAL MECHANICS
|
|
1.
|
Organoleptic (appearance, odor, flavor)
|
Organoleptic
|
-
|
|
2.
|
Impurities (sand)
|
AOAC 920.46 (2011)
|
0.02%
|
|
II. QUALITY INGREDIENTS
|
|
3.
|
Độ ẩm
|
TCVN 4326 :2001
|
% wt
|
|
4.
|
Protein thô
|
TCVN 4328-1:2007
|
% wt
|
|
5.
|
Protein Tiêu hóa(**)
|
AOAC 971.09 (2011)
|
0.05%
|
|
6.
|
Protein tan trong KOH(**)
|
Kjeldahl method
|
0.05%
|
|
7.
|
Nito bay hơi (TVN)
|
TCVN 3706-1990
|
mg/100g
|
|
8.
|
Nito bazo bay hơi (TVBN)
|
FAO 14/8, p.140, 1986
|
mg/100g
|
|
9.
|
Carbohydrate
|
Calculate (Included testing Carbohydrate, Fat, Protein),
Food Composition
|
Kcal/100g
|
|
10.
|
Tinh bột(**)
|
FAO, 14/7, 1986
|
0.02%
|
|
11.
|
Béo
|
FAO 14/7 p. 212, 1986
|
%wt
|
|
12.
|
Hàm lượng xơ thô
|
TCVN 4329: 2007
|
%wt
|
|
13.
|
Độ acid(**)
|
TCVN 4589:1988
|
0.05 ml NaOH 1N/100g
|
|
14.
|
Tro tổng
|
AOAC 942.05 (2011)
|
0.02%
|
|
|
Tro tổng
|
TCVN 4327:2007
|
0.01%
|
|
15.
|
Tro không an trong HCl
|
TCVN 4327:2008
|
0.01%
|
|
16.
|
Hàm lượng chất khô(**)
|
AOAC 930.15 (2011)
|
0.02%
|
|
17.
|
Muối (NaCl)
|
AOAC 937.09 (2011)
|
0.01%
|
|
III. OTHER INGREDIENTS
|
|
18.
|
Acid amine (gồm 20 acid
amine)(**)
|
TK.EZ : faast (LCMSMS)
|
10 mg/kg
|
|
|
Glycine
|
10 mg/kg
|
|
|
Alanine
|
|
|
|
Serine
|
|
|
|
Proline
|
|
|
|
Valine
|
|
|
|
Threonine
|
|
|
|
Methionine
|
|
|
|
Trans-4-hydroxy-proline
|
|
|
|
Arginine
|
|
|
|
Aspartic acid
|
|
|
|
Glutamic acid
|
|
|
|
Cysteine
|
|
|
|
Lysine
|
|
|
|
Histidine
|
|
|
|
Tyrosine
|
|
|
|
Cystine
|
|
|
|
Leucine _ Isoleucine
|
|
|
|
Phenylalamine
|
|
|
19
|
Saturated fatty acid(**)
|
TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
20.
|
Monounsaturated fatty
acid(**)
|
TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
21.
|
Polyunsaturated fatty
acid(**)
|
TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
22.
|
Trans fat(**)
|
TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
23.
|
Omega 3(**)
|
TK.AOAC 996.06 for food TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
24.
|
Omega 6(**)
|
TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
25.
|
Omega 9(**)
|
TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
26.
|
DHA(**)
|
TK.AOAC 996.06 for food, TK.AOAC 969.33 for oil (GC/FID)
|
20mg/kg
|
|
27.
|
Cholesterol(**)
|
TK.AOAC 970.51 (LCMSMS)
|
1.0mg/kg
|
|
28.
|
Taurin(**)
|
TK. AOAC 997.05 -2002 (LCMSMS)
|
2.0mg/kg
|
|
29.
|
Urê(**)
|
TK. Appilication Note SSI – AP – LCMS 0277 – Shimadzu (LCMSMS)
|
5.0mg/kg
|
|
IV. NITRIT AND NITRAT RESIDUES
|
|
30.
|
Nitrit (NO2-)(**)
|
TK.TCVN 7767:2007
|
1 mg/Kg
|
|
31.
|
Nitrat (NO3-)(**)
|
TK.TCVN 7767:2007
|
1 mg/Kg
|
|
V. HEAVY METAL AND OTHER METALS
|
|
32.
|
Arsen (As)
|
BSEN 15510 - 2007
|
0.01 mg/Kg
|
|
33.
|
Thủy ngân (Hg)(**)
|
AOAC 974.14 (2011)
|
0.01 mg/Kg
|
|
34.
|
Cadimi (Cd)
|
AOAC 968.08
|
0.005 mg/Kg
|
|
35.
|
Chì (Pb)
|
AOAC 968.08
|
0.01 mg/Kg
|
|
36.
|
Đồng (Cu)
|
AOAC 968.08
|
0.2 mg/Kg
|
|
37.
|
Canxi (Ca)
|
AOAC 968.08
|
0.5 mg/Kg
|
|
38.
|
Selen (Se)
|
BSEN 15510 - 2007
|
0.01 mg/Kg
|
|
39.
|
Kali (K)
|
AOAC 968.08
|
0.5 mg/Kg
|
|
40.
|
Magie (Mg)
|
AOAC 968.08
|
0.5 mg/Kg
|
|
41.
|
Mangan (Mn)
|
AOAC 968.08
|
0.5 mg/Kg
|
|
42.
|
Sắt (Fe)
|
AOAC 968.08
|
0.5 mg/Kg
|
|
43.
|
Natri (Na)
|
AOAC 968.08
|
0.5 mg/Kg
|
|
44.
|
Antimo (Sb)
|
BSEN 15510 - 2007
|
0.01 mg/Kg
|
|
45.
|
Kẽm (Zn)
|
AOAC 968.08
|
0.5 mg/Kg
|
|
46.
|
Arsen (As)
|
BSEN 15510 - 2007
|
0.01 mg/Kg
|
|
VI. ANTIBIOTIC RESIDUES
|
|
47.
|
Chloramphenicol
|
LC/MS/MS
|
0.1mg/kg
|
|
48.
|
Fluoro-quinolones
|
LC/MS/MS
|
|
|
|
Ciprofloxacin
|
10.0mg/kg
|
|
|
Enrofloxacin
|
10.0mg/kg
|
|
|
Difloxacin
|
10.0mg/kg
|
|
|
Sarafloxacin
|
10.0mg/kg
|
|
|
Norfloxacin
|
10.0mg/kg
|
|
|
Danofloxacin
|
10.0mg/kg
|
|
|
Ofloxacin
|
10.0mg/kg
|
|
|
Flumequine
|
100mg/kg
|
|
|
Oxolinic acid
|
100mg/kg
|
|
49.
|
Malachite green
|
LC/MS/MS
|
1.0mg/kg
|
|
50.
|
Leucomalachite green
|
LC/MS/MS
|
1.0mg/kg
|
|
51.
|
Nitrofuran và các dẫn
xuất (4 dẫn xuất)
|
LC/MS/MS
|
1.0mg/kg
|
|
|
AOZ (3-amino-2-
oxazolidinone)
|
1.0mg/kg
|
|
|
AMOZ ( 3-amino-5-
morpholinomethyl-
1,3-oxazolidin-2-one)
|
1.0mg/kg
|
|
|
AHD (1-aminohydrantoin)
|
1.0mg/kg
|
|
|
SEM ( Semicarbazide)
|
1.0mg/kg
|
|
52.
|
Crystal Violet
|
LC/MS/MS
|
1.0mg/kg
|
|
53.
|
Leucocrystal Violet
|
1.0mg/kg
|
|
54.
|
Họ Tetracyline
|
-
|
|
|
Tetracyclin
|
100mg/kg
|
|
|
Chlortetracyclin
|
100mg/kg
|
|
|
Oxytetracyclin
|
LC/MS/MS
|
100mg/kg
|
|
55.
|
Florfenicol
|
100mg/kg
|
|
56.
|
Họ Sulfonamides
|
|
|
|
Sulfamethoxazole
|
50.0mg/kg
|
|
|
Sulfadicine
|
50.0mg/kg
|
|
|
Sulfadiazine
|
LC/MS/MS
|
50.0mg/kg
|
|
|
Sulfathiazole
|
50.0mg/kg
|
|
|
Sulfamidine
|
50.0mg/kg
|
|
57.
|
Trifluralin
|
0.2mg/kg
|
|
58.
|
Ethoxyquin
|
10.0mg/kg
|
|
59.
|
Beta-Lactamines
|
TK.Analytical Chimica Acta 520 ( 2004), p14-32, 590 – 3722 EN, Agilent (LCMSMS)
|
|
|
|
Amipicillin
|
100mg/kg
|
|
|
Amoxycillin
|
100mg/kg
|
|
|
Benxylpenicillin
|
100mg/kg
|
|
60.
|
Streptomycin(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
100mg/kg
|
|
61.
|
Spiramycin(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
50.0mg/kg
|
|
62.
|
Gentamycin(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
50.0mg/kg
|
|
63.
|
Tylosin(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
50.0mg/kg
|
|
64.
|
Lincomycin(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
50.0mg/kg
|
|
65.
|
Họ Nitroimidazole(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
|
|
|
Ronidazole(**)
|
10.0mg/kg
|
|
|
Omidazole(**)
|
10.0mg/kg
|
|
|
Metronidazole(**)
|
10.0mg/kg
|
|
|
Ipronidazole(**)
|
10.0mg/kg
|
|
|
Dimetridazole(**)
|
10.0mg/kg
|
|
|
Tinidazole(**)
|
10.0mg/kg
|
|
VII. PLANT PROTECTION DRUG RESIDUES
|
|
66.
|
Carbamate plant protection drug residues
|
TK.AOAC 2007.01 (LCMSMS)
|
|
|
|
Isoprocarb
|
0.01mg/kg
|
|
|
Aldicarb sulfone
|
0.01mg/kg
|
|
|
Aldicarb
|
0.01mg/kg
|
|
|
Aldicarb sulfoxide
|
0.01mg/kg
|
|
|
Propoxur
|
0.01mg/kg
|
|
|
Carbofuran
|
0.01mg/kg
|
|
|
Carbaryl
|
0.01mg/kg
|
|
|
Methomyl
|
0.01mg/kg
|
|
|
Oxamyl
|
0.01mg/kg
|
|
|
Thiodicarb
|
0.01mg/kg
|
|
|
Methiocarb
|
0.01mg/kg
|
|
|
Fenobucarb
|
0.01mg/kg
|
|
|
Propoxur
|
0.01mg/kg
|
|
|
Carbofuran-3-Hydroxy
|
0.01mg/kg
|
|
67.
|
Clo plant protection drug residues
|
TK.AOAC 2007.01 (GCMS)
|
-
|
|
|
2,4'-DDD
|
0.1mg/kg
|
|
|
4,4'-DDD
|
0.1mg/kg
|
|
|
2,4'-DDE
|
0.1mg/kg
|
|
|
4,4'-DDE
|
0.1mg/kg
|
|
|
2,4'-DDT
|
0.1mg/kg
|
|
|
4,4'-DDT
|
0.1mg/kg
|
|
|
Alpha-Lindan
|
0.1mg/kg
|
|
|
Gamma-Lindan
|
0.1mg/kg
|
|
|
Beta-Lindan
|
0.1mg/kg
|
|
|
Isodrin
|
0.1mg/kg
|
|
|
Aldrin
|
0.1mg/kg
|
|
|
Dieldrin
|
0.1mg/kg
|
|
|
Endrin
|
0.1mg/kg
|
|
|
Hexachloro-Benzene
|
0.1mg/kg
|
|
|
Heptachlor
|
0.1mg/kg
|
|
|
Heptachlor epoxide
|
0.1mg/kg
|
|
|
Endosulfan I
|
0.1mg/kg
|
|
|
Endosulfan II
|
0.1mg/kg
|
|
68.
|
Phosphor plant protection drug residues
|
TK.AOAC 2007.01 (GCMS)
|
-
|
|
|
Diazinon
|
0.1mg/kg
|
|
|
Parathion Methyl
|
0.1mg/kg
|
|
|
Malathion
|
0.1mg/kg
|
|
|
Chlorpyrifos
|
0.1mg/kg
|
|
|
Parathion ethyl
|
0.1mg/kg
|
|
|
Bromophos methyl
|
0.1mg/kg
|
|
|
Bromophos ethyl
|
0.1mg/kg
|
|
|
Ethion
|
0.1mg/kg
|
|
69.
|
Chrysanthemum plant protection drug residues
|
TK.AOAC 2007.01 (GCMS)
|
-
|
|
|
Cypermethrin
|
0.1mg/kg
|
|
|
Deltamethrin
|
0.1mg/kg
|
|
|
Permethrin
|
0.1mg/kg
|
|
|
Fenvalerate
|
0.1mg/kg
|
|
|
Resmethrine
|
0.1mg/kg
|
|
|
Fenthropathrine
|
0.1mg/kg
|
|
VIII. VITAMIN
|
|
70.
|
Vitamin A(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/kg
|
|
71.
|
Vitamin D3(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/kg
|
|
72.
|
Vitamin E(**)
|
TK.AOAC 992.06:2011 (HPLC.UV)
|
0.1mg/kg
|
|
73.
|
Vitamin C
|
Ref Journal of Chromatography A UHPLC-DAD
|
1.0mg/kg
|
|
74.
|
Vitamin B1
|
Ref Journal of Chromatography A UHPLC-DAD
|
0.1mg/kg
|
|
75.
|
Vitamin B2
|
Ref Journal of Chromatography A UHPLC-DAD
|
0.1mg/kg
|
|
76.
|
Vitamin B3
(nicotinamide)
|
Ref Journal of Chromatography A UHPLC-DAD
|
0.1mg/kg
|
|
77.
|
Vitamin B5
(acid pantothenic)
|
Ref Journal of Chromatography A UHPLC-DAD
|
0.1mg/kg
|
|
78.
|
Vitamin B6
|
Ref Journal of Chromatography A UHPLC-DAD
|
0.1mg/kg
|
|
79.
|
Vitamin B9
(floic acid)
|
Ref Journal of Chromatography A UHPLC-DAD
|
0.1mg/kg
|
|
80.
|
Vitamin B12
|
Ref Journal of Chromatography A UHPLC-DAD
|
0.1mg/kg
|
|
81.
|
Biotin(**)
|
TK.AOAC 985.33:2011 (HPLC-UV)
|
0.1mg/kg
|
|
IX. ADDITIVES
|
|
82.
|
Acid citric (E330)
|
Ref Megazyme International Ireland 2012
UHPLC-DAD
|
20.0mg/kg
|
|
83.
|
Acid Tartaric (E334)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
84.
|
Acid malic (E296)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
85.
|
Acid fumaric (E297)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
86.
|
Acid lactic (E270)(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
87.
|
Acid ascorbic
/Natri ascorbate
|
Ref Megazyme International Ireland 2012
UHPLC-DAD
|
1.0mg/kg
|
|
88.
|
Aicd propionic(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
89.
|
Aicd fomic(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
90.
|
Acid acetic
/Natri acetate(**)
|
TK. US EPA method 300.00(IC)
|
20.0mg/kg
|
|
91.
|
Natri benzoate
/ Acid benzoic
|
Ref Journal of chromatography A, 1073(2005) 393 – 397
UHPLC-DAD
|
10mg/kg
|
|
92.
|
Kali sorabte/ Acid sorbic
|
Ref Megazyme International Ireland 2012
UHPLC-DAD
|
10mg/kg
|
|
93.
|
Benzoyl peroxyd(**)
|
(HPLC/UV)
|
10.0mg/kg
|
|
94.
|
Paraben(**)
|
TK. AOAC 983.16 (HPLC/UV)
|
|
|
|
Butylparaben
(Butyl-4-hydroxy
benzoate)(**)
|
10.0mg/kg
|
|
|
Ethylparaben
(Ethyl-4-hydroxy
benzoate)(**)
|
10.0mg/kg
|
|
|
Methylparaben
(Methyl-4-hydroxy
benzoate)(**)
|
10.0mg/kg
|
|
|
Propylparaben
(Propyl-4-hydroxy
benzoate)(**)
|
10.0mg/kg
|
|
|
Heptylparaben
(Heptyl-4-hydroxy
benzoate)(**)
|
10.0mg/kg
|
|
95.
|
Alpha-Tocopherol(**)
|
TK : AOAC 992.06 (HPLC/UV)
|
0.1mg/kg
|
|
96.
|
BHA (Butylated
hydroxyanisol)(**)
|
TK : AOAC 983.15 (HPLC/UV)
|
5.0mg/kg
|
|
97.
|
BHT (Butylated
hydroxytoluene)(**)
|
TK : AOAC 983.15 (HPLC/UV)
|
5.0mg/kg
|
|
98.
|
TBHQ (Tert-Butyl
hydroquinone)(**)
|
TK : AOAC 983.15 (HPLC/UV)
|
5.0mg/kg
|
|
X. GROWTH STIMULATION_ HORMON
|
|
99.
|
Beta agonist
|
LC/MS/MS
|
|
|
|
Salbutamol
|
LC/MS/MS
|
1.0mg/kg
|
|
|
Clenbuterol
|
LC/MS/MS
|
1.0mg/kg
|
|
|
Ractopamine
|
LC/MS/MS
|
1.0mg/kg
|
|
100.
|
Dexamethasone(**)
|
TK. Journal of chromatoghaphy B, volume 862, issue 1-2, p119 -124 (LCMSMS)
|
0.30µg/kg
|
|
101.
|
Hormons(**)
|
TK. CLG – AMG -1.03, USDA (LCMSMS)
|
|
|
|
Progesterol(**)
|
50.0µg/kg
|
|
|
Estradiol(**)
|
50.0µg/kg
|
|
|
Testosterone(**)
|
50.0µg/kg
|
|
|
Dietylstylbestrole(**)
|
50.0µg/kg
|
|
XI. TOXIN
|
|
102.
|
Aflatoxin Tổng(**)
|
TK.AOAC 991.31 (LC/MS/MS)
|
1.0µg/kg
|
|
103.
|
Aflatoxin/chất
(B1, B2, G1, G2)(**)
|
TK.AOAC 991.31(LC/MS/MS)
|
1.0µg/kg
|
|
104.
|
Ochratoxin A(**)
|
TK. AOAC 2000.09(LC/MS/MS)
|
1.0µg/kg
|
|
105.
|
Deoxynivalenol
(DON)(**)
|
TK.AOAC 986.18 (LC/MS/MS)
|
100µg/kg
|
|
106.
|
Zearalenone(**)
|
TK .Analytical Chimica Acta 487, p137-143 (LC/MS/MS)
|
1.0µg/kg
|
|
107.
|
Melamine(**)
|
TK. FDA 4396 (LC/MS/MS)
|
100µg/kg
|
|
XII. MICROBIOLOGY
|
|
108.
|
Enzyme lipase(**)
|
PP định phân acid béo
|
_
|
|
109.
|
Aspergillus(**)
|
Định danh nấm mốc, ISO 215272 : 2008
|
|
|
110.
|
Xác định vi khuẩn
khử sulfit phát triển
trong điều kiện kỵ khí(*)
|
ISO 15213: 2003
|
10 CFU/g
|
|
111.
|
Phát hiện Vibrio cholerae -
Phương pháp phát hiện
Vibrio spp,có khả năng
gây bệnh đường ruột (*)
|
TCVN 7905-1:2008, (ISO 21872-1:2007 E)
|
/25g
|